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• W2057180561 abstract "A staggered conformation was established for (CH3)3N · BF3 and (CH3)3N · BCl3 by an electron diffraction analysis. The following main geometrical parameters were obtained.t001. 1Parameter(CH3)3N · BF3(CH3)3N · BCl3ra(B-X)1.354 ± 0.006 Å1.839 ± 0.004 Å∠X-B-X113.1 ± 0.9°110.8 +- 0.3°ra(N-C)1.468 ± 0.010 Å1.495 ± 0.004 Å∠C-N-C108.5 ± 0.7°108.7 +- 0.5°ra(B-N)1.664± 0.011 Å1.659 ± 0.006 Å The structural changes, observed primarily in the acceptor parts, provide further evidence that BCl3, is a stronger acceptor than BF3. The structure of the chlorine derivative and analogy with respective Al-N complexes support the early suggestion for a long B-N bond in (CH3)3N · B(CH3)3. t001. 1" @default.
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• W2057180561 date "1977-06-01" @default.
• W2057180561 modified "2023-09-26" @default.
• W2057180561 title "Electron diffraction investigation of the molecular structures of two trimethylamine-boron halide adducts in the vapour phase" @default.
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• W2057180561 doi "https://doi.org/10.1016/0022-2860(77)85036-9" @default.
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