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• W2057182302 endingPage "4181" @default.
• W2057182302 startingPage "4168" @default.
• W2057182302 abstract "A new Schiff base, (pyridin-2-yl)-N-(3,5-di(pyridin-2-yl)-4H-1,2,4-triazol-4-yl)methanimine, (L), was synthesized. Reaction of [(η6-arene)Ru(µ-Cl)Cl]2 and [Cp*M(µ-Cl)Cl]2 (M = Rh and Ir) with one equivalent of L in the presence of NH4PF6 in methanol yielded dinuclear complexes, [(η6-arene)2Ru2(L-OH)Cl](PF6)2 {arene = C6H6 (1), p-iPrC6H4Me (p-cymene) (2) and C6Me6 (3)}, and [Cp*2M2(L-OH)Cl](PF6)2 [M = Rh (4) and Ir (5)], respectively, leading to the formation of five new chiral complexes with –OH on the azomethine carbon. L is a pentadentate ligand where one of the metal centers is coordinated to two nitrogen atoms in a bidentate chelating fashion while the other metal is bonded tridentate to three nitrogen atoms. Although the ligand is neutral before coordination, after complexation it is anionic (uni-negative) with negative charge on the azo nitrogen {see the structures: N(5) in 2[PF6]2 and N(3) for 4[PF6]2}. The complexes have been characterized by various spectroscopic methods including infrared and 1H NMR and the molecular structures of the representative complexes are established by single-crystal X-ray diffraction studies." @default.
• W2057182302 created "2016-06-24" @default.
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• W2057182302 date "2011-11-18" @default.
• W2057182302 modified "2023-09-26" @default.
• W2057182302 title "Hydroxylation of azomethine carbon: isolation of complexes of η5 and η6-cyclic hydrocarbon platinum group metals with a new Schiff-base ligand" @default.
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• W2057182302 doi "https://doi.org/10.1080/00958972.2011.636427" @default.
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