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• W2057186736 startingPage "1778" @default.
• W2057186736 abstract "Ceramic pigments based on the Cr-doped malayaite structure were synthesized by solid state reaction and characterized by optical spectroscopy and combined X-ray and neutron powder diffraction in order to elucidate the still unclear chromium substitution mechanisms. The results show that coloration is actually due to simultaneous occurrence of Cr4+ and Cr3+ ions in the crystal lattice. Spectroscopy data confirm that Cr4+ is replacing Sn4+ in the octahedral site and, in minor amount, Si4+ in the tetrahedral site. In addition, neutron powder diffraction data suggest that Cr3+ substitution for octahedral Sn4+ is charge balanced by the formation of oxygen vacancies with no preference over the different oxygen sites. Upon incorporation of Cr ion, the SnO6 octahedra exhibit an off-centre displacement of central cation which in turn induces a rearrangement of both the octahedral and tetrahedral coordination shells." @default.
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• W2057186736 date "2009-08-01" @default.
• W2057186736 modified "2023-09-30" @default.
• W2057186736 title "Malayaite ceramic pigments: A combined optical spectroscopy and neutron/X-ray diffraction study" @default.
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• W2057186736 doi "https://doi.org/10.1016/j.materresbull.2009.03.006" @default.
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