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- W2057256105 abstract "Abstract Facile chemical synthesis of the natural chiral‐pool‐derived host 1 and its subsequent crystallization (“supramolecular synthesis”) from different solvents yielded crystalline assemblies. Crystal structure determinations of five of the so formed solvent‐inclusion compounds ( 1 a – 1 e ) reveal hexagonal symmetries in four cases. The structural characteristics of these chiral host–guest ensembles with varying stoichiometries can be best described as assemblies formed through intra‐pair hydrogen bridges of host molecules into Piedfort pairs of differing complexity. Hitherto undescribed, these Piedfort pairs also form even larger regular assemblies that we designate “Big Mac”‐like shapes. In the only nonhexagonal case, six independent host molecules form a huge supramolecular analogue of [6]benzocyclophane, also known as [6]chochin, extending this giant supermolecule through intermolecular hydrogen bonds into macroscopic (mm‐size) dimensions. As all these crystals are inherently chiral, and new model systems for solid‐state applications can be envisaged." @default.
- W2057256105 created "2016-06-24" @default.
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- W2057256105 date "2003-07-22" @default.
- W2057256105 modified "2023-10-11" @default.
- W2057256105 title "Supramolecular[6]Chochin and“Big Mac” Made from Chiral Piedfort Assemblies" @default.
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- W2057256105 doi "https://doi.org/10.1002/chem.200304969" @default.
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