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- W2057376510 abstract "Abstract The chemical shifts of 99m Tc core-electron binding energies were measured in solid samples by means of the internal conversion electron spectroscopy (ICES) method. Technetium chelates with citric acid, DTPA, EDTA and ethylenediamine- N , N ′-tetraacetohydroxamic acid (EDTAHA) as ligands were prepared in solution at (2–4) × 10 −7 M Tc concentration (no-carrier-added). The samples for ICES measurements were made by evaporation of the solution in vacuum to dryness. The following chemical shifts ΔE B [K 99m TcO 4 - 99m Tc(chelate)] were found in the systems investigated: 1.9 and 4.1 eV for 99m Tc(Sn)citr; 2.1, 3.2 and 4.3 eV for 99m Tc(Sn)DTPA; 1.9 and 3.6 eV for 99m Tc(Sn)EDTA; 1.8 and 3.3 eV for 99m Tc(Sn)EDTAHA. Standard deviations of the shifts are 0.2 eV. These shifts were compared with those of inorganic technetium oxocompounds and correlated with oxidation states via a potential model. It was concluded, that these shifts refer to technetium oxidation states in chelates as follows: 1.8–2.1 eV to 99m Tc(V), 3.2–3.6 eV to 99m Tc(IV) and 4.1–4.3 eV to 99m Tc(III)." @default.
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- W2057376510 date "1986-01-01" @default.
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- W2057376510 title "Oxidation states of 99mTc in technetium chelates studied by the ICES method" @default.
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- W2057376510 doi "https://doi.org/10.1016/0883-2889(86)90009-2" @default.
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