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- W2057388629 abstract "Abstract Chemical reduction of (C5H4-t-Bu)2Zr(CH2PPh2)2 (1) was monitored by ESR and 1H NMR spectroscopy. A labile ZrIII species, (C5H4-t-Bu) Zr(CH 2 P Ph2)2 (2), was first characterized by its ESR signal (triplet of quintet; a(1H) 3.5 G; a(31P) 11.0 G). Evolution of 2 at room temperature afforded another species 3 (doublet of doublet, a1H) 6.0 G; a(31P) 25.5 G), which was shown by its reaction with CH3I to be a hydride (by formation of CH4) to contain a ZrCH 2 P Ph2 moiety (by formation of PPh2MeEtI), and formulated as (C5H4-t-Bu) ZrH(CH 2 P Ph2) (3)." @default.
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- W2057388629 date "1989-05-01" @default.
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- W2057388629 title "Formation of a hydrido diphenylphosphinomethylzirconium(III) species by reduction of (C5H4-t-Bu)2Zr(CH2PPh2)2" @default.
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- W2057388629 doi "https://doi.org/10.1016/0022-328x(89)80127-5" @default.
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