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• W2057808534 startingPage "125" @default.
• W2057808534 abstract "A fluorous linker-assisted synthetic protocol has been developed for preparation of sclerotigenin-type benzodiazepine-quinazolinone library containing 144 analogues. Amide coupling of fluorous trimethoxybenzyl (TMB)-protected amino esters with anthranilic acids followed by base-promoted cyclizations afforded 4-benzodiazepine-2,5-diones. Further derivatization of benzodiazepinediones by reacting with azidobenzoyl chlorides, cyclization, and fluorous linker cleavage afforded the desired compound library. The reaction intermediates were purified by fluorous solid-phase extraction (F-SPE) and final products were further purified by prep-HPLC." @default.
• W2057808534 created "2016-06-24" @default.
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• W2057808534 date "2009-12-15" @default.
• W2057808534 modified "2023-09-26" @default.
• W2057808534 title "Fluorous Synthesis of Substituted Sclerotigenin Library" @default.
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• W2057808534 doi "https://doi.org/10.1021/cc9001636" @default.
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• W2057808534 hasPublicationYear "2009" @default.
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