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• W2057846231 abstract "High-resolution 13C NMR spectra of a variety of (1→3)-β-D-glucans were recorded in the solid state after lyophilization from DMSO solution in order to study resulting conformations free from the triple-helix conformation. Lyophilization from DMSO solution caused conformational change of laminaran from Laminaria species (‾Dp=38) from the triple helix to the oligomer-type form (form I). On the contrary, single-chain conformation (form II) of high molecular-weight curdlan was unchanged before and after lyophilization from DMSO solution. Further, DMSO induced conformational change of both single-chain (form II) and triplehelical (form III) conformations of acid-degraded curdlan (‾Dp=14) to the form I. These findings support our view that the single-chain conformation is a major form in curdlan powder. We found that these three forms are distinguished by either the 13C spin-lattice relaxation times (T1C’s) of the laboratory frame or proton spin-lattice relaxation times in the rotating frame (T1ρH). In particul..." @default.
• W2057846231 created "2016-06-24" @default.
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• W2057846231 date "1989-02-01" @default.
• W2057846231 modified "2023-10-13" @default.
• W2057846231 title "High-Resolution¹³C NMR Study of (1→3)-β-D-Glucans in the Solid State: DMSO-Induced Conformational Change and Conformational Characterization by Spin-Relaxation Measurements" @default.
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• W2057846231 doi "https://doi.org/10.1246/bcsj.62.392" @default.
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