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- W2057898601 abstract "Es wurden zwei stellungsisomere Reineckesalzanaloga, [Cr(NCS)4(m-Toluylendiamin)2]− und [Cr(NCS)4(p-Toluylendiamin)2]−, durch eine Substitutionsreaktion aus entwässertem K3[Cr(NCS)6] und meta-, bzw. para-Toluylendiamin, ohne Verwendung von Lösungsmitteln, erhalten. Die Herstellung von 18 Salzen rnit den Chlorhydraten der Alkaloide und mit Kobalt (111)-amin-Komplexen bestätigt die Zusammensetzung der erwähnte Komplexanionen. Zur Klärung einiger Strukturfragen und thermischer Stabilitätsprobleme wurden spektrophotometrische Untersuchungen im sichtbaren und IR-Bereich des Spektrums und derivatographische Untersuchungen durchgeführt. New Position Isomeric Analoga of Reinecke Salt with m- and p-Tolylenediamine Two position isomeric Reinecke salt analogous complexes, [Cr(NCS)4(m-TolyIenediamine)2]− and [Cr(NCS)4(p-Tolylenediamine)2]−, were obtained by means of substitution reactions of anhydrous K3[Cr(NCS)6] with meta and para tolylenediamine, respectively, without solvent. The formulae of the new complex anions were established by preparation of 18 new derivatives with the hydrochlorides of some alksloides, and cobalt(III) amine bases. From electronic and IR spectral data some structural problems are solved. The thermal stability of some complexes was discussed on the basis of derivatographic analysis." @default.
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- W2057898601 date "1976-06-01" @default.
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- W2057898601 title "Neue stellungsisomere Reineckesalzanaloga mit Meta- und Para-Toluylendiamin" @default.
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- W2057898601 doi "https://doi.org/10.1002/zaac.19764230311" @default.
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