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- W2057899501 abstract "Abstract A mass spectrometer for isotopic analysis of solid uranium samples has been constructed and evaluated. This system employs the fluorinating agent chlorine trifluoride (ClF 3 ) to convert solid uranium samples into their volatile uranium hexafluorides (UF 6 ). The majority of unwanted gaseous byproducts and remaining ClF 3 are removed from the sample vessel by condensing the UF 6 and then pumping away the unwanted gases. The UF 6 gas is then introduced into a quadrupole mass spectrometer and ionized by electron impact ionization. The doubly charged bare metal uranium ion (U 2+ ) is used to determine the U 235 /U 238 isotopic ratio. Precision and accuracy for several isotopic standards were found to be better than 12%, without further calibration of the system. The analysis can be completed in 25 min from sample loading, to UF 6 reaction, to mass spectral analysis. The method is amenable to uranium solid matrices, and other actinides." @default.
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- W2057899501 date "2001-07-01" @default.
- W2057899501 modified "2023-09-25" @default.
- W2057899501 title "Analysis of solid uranium samples using a small mass spectrometer" @default.
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- W2057899501 doi "https://doi.org/10.1016/s0584-8547(01)00235-x" @default.
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