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- W2058021284 abstract "High-temperature studies of mercuric iodide (HgI/sub 2/) involving differential scanning calorimetry (DSC), Raman spectroscopy, and x- ray powder diffraction have failed to confirm the existence of a red-colored tetragonal high-temperature phase called ..cap alpha.. '-HgI/sub 2/ reported by S.N. Toubektsis et al., (S.N. Toubektsis, E.K. Polychroniadis, and N.A. Economou, J. Appl. Phys., 58(5) (1985) 2070), using DSC measurements. The multiple DSC peaks near melting reported by Toubektsis are found by the present authors only if the sample is heated in a stainless-steel container. Using a Pyrex container or inserting a platinum foil between the HgI/sub 2/ and the stainless-steel container yields only one sharp, single DSC peak at the melting point. The nonexistence of the ..cap alpha..' phase is confirmed by high- temperature x-ray diffraction and Raman spectroscopy performed in the vicinity of the melting point which clearly indicate the existence of the yellow orthorhombic ..beta..-HgI/sub 2/ phase only. The experimental high-temperature DSC, Raman, and x-ray diffraction data are presented and discussed. 14 refs., 8 figs., 2 tabs." @default.
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- W2058021284 date "1989-11-01" @default.
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- W2058021284 title "A study of mercuric iodide near melting using differential scanning calorimetry, Raman spectroscopy and X-ray diffraction" @default.
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- W2058021284 doi "https://doi.org/10.1016/0168-9002(89)91348-x" @default.
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