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• W2058049802 abstract "Abstract The thermal decomposition processes taking place in the solid state mixture of NiC 2 O 4 · 2H 2 O–MgC 2 O 4 · 2H 2 O (2:1 mole ratio) have been investigated in air using TG–DTG, differential scanning calorimetry (DSC) and XRD techniques. The decomposition proceeded through four well-defined steps while TG curves closely corresponded to the theoretical mass loss. The result of XRD showed the well-crystallized MgNi 2 O 3 formed in the sample calcined at 600 °C for 2 h. The activation energies for the decompositions of NiC 2 O 4 and MgC 2 O 4 were calculated through the Ozawa and Kissinger–Akahira–Sunose (KAS) methods, and the possible conversion functions have been estimated through the comparative method. The activation energies for the decompositions of NiC 2 O 4 were 151.05 kJ/mol (KAS method) and 152.6 kJ/mol (Ozawa method), and the activation energies for the decompositions of MgC 2 O 4 were 204.74 kJ/mol (KAS method) and 205.72 kJ/mol (Ozawa method). The possible conversion function for the decomposition of NiC 2 O 4 and MgC 2 O 4 kept to the conversion function of “ Nucleation and Growth ” and “ phase boundary reaction ”, respectively." @default.
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• W2058049802 date "2006-03-01" @default.
• W2058049802 modified "2023-10-17" @default.
• W2058049802 title "Synthesis of MgNi2O3 and kinetics of thermal decomposition of the oxalate precursor" @default.
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• W2058049802 doi "https://doi.org/10.1016/j.jaap.2005.06.007" @default.
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