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- W2058171900 abstract "This paper assesses the effectiveness of zone refining and recrystallization from solution of three materials exhibiting allotropie phase changes,n-hexatriacontane cholesteryl stearate andp-azoxyanisole. Purity determinations are performed by means of a quantitative interpretation of the shape of DTA peaks following the procedure of Davis and Porter. It is concluded that zone refining ofn-hexatriacontane is far more effective than recrystallization from solution. The results for cholesteryl stearate andp-azoxyanisole are more complex: Zone refining alone is in both cases somewhat more effective than recrystallization from solution. Evidence is presented which demonstrates in both substances the presence of at least one impurity component which increases the solid/smectic and solid/nematic transition temperatures, respectively. Such impurities are removed only very slowly by zone refining, but apparently even much slower, if at all, by recrystallization." @default.
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- W2058171900 title "The effect of zone refining and recrystallization on organic materials exhibiting allotropic phase transitions" @default.
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