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• W2058379316 startingPage "1149" @default.
• W2058379316 abstract "LiNizMn1 –zO2 cathode materials have been prepared using a ‘chimie douce’ route for 0.5 ⩽z⩽1 Coprecipitation of hydroxides is followed by drying and heating at 700 °C for 5 h under oxygen flow. Because of the high reactivity of the coprecipitates, the preparation time is shorter than for the classical powder mixing and heating methods used generally, and materials with 0.5⩽z⩽1 are obtained easily. DTA-TG and XRD studies have been performed for each composition. The LiNizMn1 –zO2 crystallinity deteriorates progressively when the manganese content is increased, but in contrast to the pure LiNiO2 compound, partial manganese substitution removes the lithium deficiency. Moreover, owing to the ease of oxidation of manganese ions, partially substituted compounds can be obtained at lower temperature than for pure LiNiO2. However, manganese substitution in LiNiO2 deteriorates the electrochemical capacity and reversibility of this compound. This is probably due to the large difference between the structures of nickel and manganese lithium oxides, which produces increasing disorder between layers when the Mn content is increased." @default.
• W2058379316 created "2016-06-24" @default.
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• W2058379316 date "1996-01-01" @default.
• W2058379316 modified "2023-10-07" @default.
• W2058379316 title "Preparation by a ‘chimie douce’ route and characterization of (LiNi_zMn_{1 –z}O₂)(0.5⩽z⩽1) cathode materials" @default.
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• W2058379316 doi "https://doi.org/10.1039/jm9960601149" @default.
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