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• W2058523786 abstract "Abstract The new high‐pressure borate HP‐Cs 1− x (H 3 O) x B 3 O 5 ( x =0.5–0.7) was synthesized under high‐pressure/high‐temperature conditions of 6 GPa/900 °C in a Walker‐type multianvil apparatus. The compound crystallizes in the monoclinic space group C 2/ c ( Z =8) with the parameters a =1000.6(2) , b =887.8(2), c =926.3(2) pm, β =103.1(1)°, V =0.8016(3) nm 3 , R 1=0.0452, and wR 2=0.0721 (all data). The boron–oxygen network is analogous to those of the compounds HP‐MB 3 O 5 , (M=K, Rb) and exhibits all three structural motifs of borates—BO 3 groups, corner‐sharing BO 4 tetrahedra, and edge‐sharing BO 4 tetrahedra—at the same time. Channels inside the boron–oxygen framework contain the cesium and oxonium ions, which are disordered on a specific site. Estimating the amount of hydrogen by solid‐state NMR spectroscopy and X‐ray diffraction led to the composition HP‐Cs 1− x (H 3 O) x B 3 O 5 ( x =0.5–0.7), which implies a nonzero phase width." @default.
• W2058523786 created "2016-06-24" @default.
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• W2058523786 date "2014-02-26" @default.
• W2058523786 modified "2023-10-18" @default.
• W2058523786 title "Oxonium Ions Substituting Cesium Ions in the Structure of the New High-Pressure Borate HP-Cs_1−<i>x</i>(H₃O)_<i>x</i>B₃O₅(<i>x</i>=0.5-0.7)" @default.
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• W2058523786 doi "https://doi.org/10.1002/chem.201303550" @default.
• W2058523786 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/24574126" @default.
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