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- W2058756443 abstract "The chemical synthesis of appropriately protected partially-deuterated 2′(R/S),3′,5′(R/S)-2H3-2′-deoxyribonucleoside blocks [∼43 atom % 2H at C5′(R), ∼57 atom % 2H at C5′(S); ∼15 atom % 2H at C2′(R), ∼85 atom % 2H at C2′(S) and >99 atom % 2H at C3′] is reported. The availability of these deuterium labelled blocks on large scale has enabled the chemical assemblage of the deuterio isotopomeric 12mer DNA duplex by standard solid-phase synthesis protocol in order to demonstrate the usefulness of the new “NMR-window III” approach (see the following paper)." @default.
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- W2058756443 date "1998-11-01" @default.
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- W2058756443 title "Synthesis of partially-deuterated 2′-deoxyribonucleoside blocks and their incorporation into an oligo-DNA for simplification of overcrowding and selective enhancement of resolution and sensitivity in the 1H-NMR spectra" @default.
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- W2058756443 doi "https://doi.org/10.1016/s0040-4020(98)00905-3" @default.
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