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- W2058871880 abstract "ZSM-5 membranes were prepared on mullite supports by a static secondary hydrothermal synthesis without applying organic structure directing agents. The ZSM-5 membrane had Si/Al ratio of 13.1 and selectively permeated water from the binary acetic acid/water mixtures and the quaternary acetic acid/ethanol/water/ethyl acetate (HAc/EtOH/H2O/AcOOEt) mixtures by pervaporation. The deviation of the dehydration performance of the membranes prepared in different batch was small, suggesting the high reproducibility of the synthesis. Part of the Na+ in the ZSM-5 membrane was replaced to H+ during the dehydration of acetic acid solution. Cation type was changed back to Na+ by immersing the membranes in 0.1 M sodium hydroxide (NaOH) or sodium chloride (NaCl) solutions. The perm-selectivity of the membranes was maintained even after applying pure HAc liquid for 77 h and applying esterification product of ethanol and acetic acid for 98 days. No change in the membrane structure was observed before and after the dehydration of acidic solutions by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis characterizations. These results confirm the high acidic stability of the membrane." @default.
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- W2058871880 date "2013-11-01" @default.
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- W2058871880 title "Dehydration of acetic acid and esterification product by acid-stable ZSM-5 membrane" @default.
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- W2058871880 doi "https://doi.org/10.1016/j.micromeso.2012.12.044" @default.
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