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- W2059093759 abstract "Reactions of [Cp∗RuCl(μ-Cl)2RuCp∗Cl] (2) with excess [MS4]2− (M W (1a or Mo (1b)) in in tetrahydrofuran at reflux afforded the trinuclear heterometallic clusters with bridging disulfide and sulfide ligands [(μ2-S2)(Cp∗Ru)2(μ3-S)(μ2-S)2MS] (M W (3a) or Mo (3b)). Clusters 3 were also obtained by treatment of an equimolar mixture of 1 and 2 with Li2S2 at room temperature. X-ray analysis was undertaken to clarify the detailed structures of clusters 3. Crystal data for 3a: monoclinic; space group, P21/c (No. 14); a = 16.460(2) A, b = 10.009(3) A and c = 16.582(2) A; β = 93.68(1)°, V = 2726(1) A3; Z = 4; Dcalc = 2.07 g cm−3; μ(Mo Kα) = 58.26 cm−1; and R(Rw) = 0.053 (0.065) for 3060 reflections (| Fo | > 3 σ (Fo)). Crystal data for 3b: monoclinic; space group, P21/c (No. 14); a = 16.530(6) A, b = 9.992(3) A and c = 16.633(6) A; β = 93.82(3)°, V = 2741(2) A3, Z = 4, Dcalc = 1.84 g cm−3; μ(Mo Kα) = 19.56 cm−1, and R(Rw) = 0.056 (0.064) for 3390 reflections (| Fo | > 3 σ (Fo)). When reacted with excess PEt3, 3a was converted into a trinuclear cluster [Cp∗Ru(PEt3)(μ2-S)2W(μ2-S)2RuCp∗(PEt3)]." @default.
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- W2059093759 date "1996-01-01" @default.
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- W2059093759 title "Trinuclear heterometallic clusters with bridging disulfide and sulfide ligands [] derived from diruthenium complex [] and [MS4]2− (M W, Mo; )" @default.
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- W2059093759 doi "https://doi.org/10.1016/0022-328x(95)05743-9" @default.
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