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- W2059096568 abstract "13C Nuclear magnetic resonance (NMR) spectra of poly (N-isopropylacrylamide) (PNiPAM) in aqueous solution and in the gel phase are measured at temperatures in the range 11.5–44°C using a ceramic rotor sealed with a rubber O-ring. In these experiments, a high resolution spectrum in the gel phase was obtained by means of the pulse saturation transfer/magic angle spinning (PST/MAS) technique and so 13C chemical shift values for all the carbons of PNiPAM were obtained. It was found that the carbonyl and methylene 13C chemical shifts change in a stepwise manner at about 32°C, the temperature at which gelation occurs. On the basis of these results, the structural change of PNiPAM in going from isotropic solution to the gel phase was discussed." @default.
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- W2059096568 date "1991-05-01" @default.
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- W2059096568 title "A 13C PST/MAS NMR study of poly (N-isopropylacrylamide) in solution and in the gel phase" @default.
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- W2059096568 doi "https://doi.org/10.1016/0022-2860(91)87113-v" @default.
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