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- W2059371034 abstract "Abstract and summary A quantitative gas liquid chromatographic (GLC) method for four organic acids‐citric, aconitic, itaconic, and citraconic acids‐in refined oils and fats was developed. After the organic acids are extracted with water from soybean oils, the extract is esterified with n‐butanol and an aliquot of the ester is subjected to GLC on a temperature‐programmed 10% DEGS column equipped with a flame ionization detector. At 20 and 30 ppm levels, recoveries of the acids from the oil varied from 95 to 100% except for itaconic acid. Citric acid content in commercial edible oils in Japan was from trace to 16 ppm. However, aconitic, itaconic, and citraconic acids were not detected." @default.
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- W2059371034 date "1977-08-01" @default.
- W2059371034 modified "2023-09-29" @default.
- W2059371034 title "Determination of citric acid and its decomposed products in edible oils by gas liquid chromatography" @default.
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- W2059371034 doi "https://doi.org/10.1007/bf02672439" @default.
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