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• W2059382830 abstract "The reduction of MoO3 into MoO2 is investigated by X-ray analysis and electron microscopy from MoO3 (010) platelets between 1000 Å and 5 mm long. In all cases, the following orientation relationship between both lattices is found: [100]2 ∥ [010]3, [122]2 ∥ [100]3, [122]2 ∥ [001]3. MoO3 crystallites twinning and misorientation are discussed in relation with the particular importance of [101]3 directions in MoO3 preserved in the transformation and becoming [010]2 of MoO2. A model for this topotactic reduction is proposed where the reaction develops layer (010)3 by layer (010)3 to form {201}2 type planes in MoO2 structure. Data on the kinetics of the boundary moving in [010]3 direction are also presented. L'étude structurale du passage de MoO3 à MoO2 a été effectuée par analyse X et microscopie électronique à partir de cristaux de MoO3 de tailles très diverses (de 1000 Å à 5 mm). Dans tous les cas, les relations structurales suivantes caractérisent la transformation: [100]2 ∥ [010]3, [122]2 ∥ [100]3, [122]2 ∥ [001]3. Le mǎclage de MoO2 et les désorientations systématiques sont discutées par rapport au rǒle particulier des directions [101]3 de MoO3, directions les mieux conservées dans la transformation et devenant [010]2 de MoO2. Un modèle pour cette réaction topotactique est proposé dans lequel les plans {201}2 de MoO2 se forment directement par la transformation successive des couches (010)3. Des données sur la cinétique du déplacement de l'interface MoO3MoO2 selon [010]3 sont aussi présentées." @default.
• W2059382830 created "2016-06-24" @default.
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• W2059382830 date "1980-08-16" @default.
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• W2059382830 title "X-ray and electron microscopy investigation of the topotactic transformation of MoO3 into MoO2" @default.
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• W2059382830 doi "https://doi.org/10.1002/pssa.2210600222" @default.
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