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- W2059625633 abstract "10-Deazaaminopterin (1) and 10-Ethyl-10-deazaaminopterin (2) labeled uniformly with 14C at the glutamate moiety were prepared by the following procedure. Uniformly labeled L-glutamic acid was converted to its dimethyl ester (3). 4-Amino-4-deoxy-10-deazapteroic acid (4) and 4-amino-4-deoxy-10-ethyl-10-deazapteroic acid (5) were converted to their respective mixed anhydrides 6 and 7 with isobutylchloroformate. Reaction of 6 and 7 with labeled dimethyl-L-glutamate gave dimethyl-10-deazaaminopterin (8) and dimethyl 10-ethyl-10-deazaaminopterin (9) respectively, which on mild alkaline hydrolysis gave the target compounds 1 and 2 in 22-25% yield, based on the amount of radiolabeled glutamic acid used." @default.
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- W2059625633 date "1987-08-01" @default.
- W2059625633 modified "2023-09-26" @default.
- W2059625633 title "Folate analogues: 27. syntheses of 14carbon-labeled 10-deazaaminopterin and 10-ethyl-10-deazaaminopterin" @default.
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- W2059625633 doi "https://doi.org/10.1002/jlcr.2580240803" @default.
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