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- W2059791545 abstract "Addition of ˙NO to dilute (ca. 10–4 mol l–1) solutions of 2,3-dimethylbuta-1,3-diene gave at least two nitroxyl radicals. The major radical, with a half-life of ca. 30 min, had an EPR spectrum with 1H hyperfine splitting of ca. 10 G from four equivalent protons. Similarly, the major nitroxyl radical formed from 2,5-dimethylhexa-2,4-diene gave a major triplet showing no resolved 1H hyperfine coupling, but satellite features from 13C (a= 10 G) from two equivalent nuclei. A minor radical with slightly different 14N coupling and a 13C splitting of 6.5 G was also detected. These radicals were very stable. On dilution of the diene, the second species was favoured over the former, and became the major component at ⩽ 10–5 mol l–1. These reactions occurred in the complete absence of ˙NO2. No radicals were detected using pure ˙NO2, but mixtures gave strong signals from nitroxyl radicals." @default.
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- W2059791545 date "1996-01-01" @default.
- W2059791545 modified "2023-09-28" @default.
- W2059791545 title "Reactions of conjugated dienes with nitrogen monoxide and dioxide" @default.
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- W2059791545 doi "https://doi.org/10.1039/ft9969201767" @default.
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