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- W2059969332 abstract "The synthesis of a new coil–rod–coil ABA triblock copolymers comprised of regioregular poly(3-hexylthiopene) (P3HT) and poly(methyl methacrylate) (PMMA) segments has been demonstrated by the combination of quasi-living Grignard metathesis (GRIM) polymerization and living anionic polymerization based on 1,1-diphenylethylene (DPE) chemistry. The method involves simple reaction steps, an in situ introduction of DPE moieties at the α,ω-ends of P3HT and the lithiation with sec-butyl lithium (sec-BuLi) to generate a macroinitiator bearing 1,1-diphenylalkyl anions, followed by cross-over to MMA. The selective α,ω-ends di-functionalization is a key step to achieve the ABA structure. The structural homogeneity of the precursor and block copolymer has been confirmed by gel permeation chromatography (GPC), GPC-right angle laser light scattering (RALLS), and nuclear magnetic resonance (NMR). The block copolymer has been fully characterized by differential scanning calorimetry (DSC), thermogravimetry analysis (TGA), Ultra-violet–visible (UV–vis) and photo luminescent (PL) spectroscopies, and atom force microscopy (AFM)." @default.
- W2059969332 created "2016-06-24" @default.
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- W2059969332 date "2009-07-01" @default.
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- W2059969332 title "Synthesis and characterization of a novel coil–rod–coil triblock copolymers comprised of regioregular poly(3-hexylthiophene) and poly(methyl methacrylate) segments" @default.
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- W2059969332 doi "https://doi.org/10.1016/j.reactfunctpolym.2008.12.004" @default.
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