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• W2060051116 abstract "A novel nanocrystalline Pb2Sn2O6 photocatalyst was prepared successfully for the first time by a hydrothermal process at 180 °C for 12 h. The samples were characterized by an x-ray diffractometer (XRD), scanning electron microscope (SEM), transmission electron microscope (TEM), surface area (BET) and ultraviolet–visible (UV–vis) spectroscopes. The results showed that the pH value played an important role in controlling the phase formation and crystallite sizes of the Pb2Sn2O6. A single phase could be obtained at a pH≥9. A possible reaction mechanism in the hydrothermal process was also proposed. The average particle size for the sample prepared at pH = 13 was only about 9 nm, and the BET surface area was as large as 76.7 m2 g−1. The N2 adsorption–desorption isotherms and pore size distribution curve demonstrate a mesoporous structure with a narrow pore size distribution. As a novel photocatalyst, the prepared Pb2Sn2O6 samples exhibit powerful photocatalytic activity for the decomposition of methyl orange under 365 nm UV light irradiation. Furthermore, it was found that the degradation process may be initiated directly by photogenerated holes rather than commonly sensed hydroxyl radicals." @default.
• W2060051116 created "2016-06-24" @default.
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• W2060051116 date "2008-11-25" @default.
• W2060051116 modified "2023-09-23" @default.
• W2060051116 title "Hydrothermal synthesis and performance of a novel nanocrystalline Pb₂Sn₂O₆photocatalyst" @default.
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• W2060051116 doi "https://doi.org/10.1088/0957-4484/19/50/505705" @default.
• W2060051116 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/19942782" @default.
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