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- W2060219152 abstract "Endothiopeptides have been obtained by using PyBOP® promoted coupling between Fmoc-protected amino monothioacids and amino acid or peptide esters. The protected endothiopeptides (Fmoc-Gly-ψ(CSNH)-Phe-OEt, Fmoc-Tyr(Bu t )-ψ(CSNH)-Gly-Gly-Phe-Leu-OBu t and Fmoc-Gln(Trt)-ψ(CSNH)-Phe-OEt) were formed (55, 45 and 37% yield) in admixture with the corresponding oxopeptides, from which they were easily separated chromatographically. Preliminary racemisation studies indicate that products of high optical purity are obtained. The mechanism for endothiopeptide formation is briefly discussed. Preparation of peptide thioamides (endothiopeptides) has been accomplished by PyBOP® promoted coupling between Fmoc amino monothioacids and amino acid or peptide esters." @default.
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- W2060219152 date "1991-12-01" @default.
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- W2060219152 title "Formation of peptide thioamides by use of Fmoc amino monothioacids and PyBOP." @default.
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- W2060219152 doi "https://doi.org/10.1016/0040-4039(91)80549-l" @default.
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