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- W2060262012 startingPage "2919" @default.
- W2060262012 abstract "The reaction of 3-iodo-3,6-dialkyl-1,2-cyclohexanedione (2) with iodine–copper(II) acetate in acetic acid–water (5:1) at 80 °C gave the respective 3-hydroxy-2,5-dialkyl-1,4-benzoquinone in 38–80% yields. On the other hand, the reaction of 2 with copper(II) acetate in acetic acid–water (10:1) under refluxing afforded the respective 3,3′-dihydroxy 2,2′,5,5′-tetraalkyl-4,4′-diphenoquinone (5) in 41–85% yields. In the case of 3-bromo-3,6-dialkyl derivative (3) with copper(II) acetate, the diphenoquinone derivatives and 3-hydroxy-2,5-dialkyl-1,4-benzoquinone were obtained." @default.
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- W2060262012 date "1989-09-01" @default.
- W2060262012 modified "2023-09-26" @default.
- W2060262012 title "A New Synthesis of 3-Hydroxy-2,5-dialkyl-1,4-benzoquinone from 3-Halo-3,6-dialkyl-1,2-cyclohexanedione Using Iodine–Copper(II) Acetate" @default.
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- W2060262012 doi "https://doi.org/10.1246/bcsj.62.2919" @default.
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