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- W2060478606 abstract "Two variations of a method for the determination of microgram amounts of thallium in biological material have been worked out. After wet combustion and separation of thallium from most interfering substances by extraction of thallic chloride with ether, the metal is estimated absorptiometrically as its dithizonate, the yield being slightly greater than theoretical (procedure A). In the presence of mercury (> i mg), cadmium, bismuth and indium (> 10 mg) high results were obtained. Other metals, halogeń, thiosulphate and thiocyanate ions did not interfere. With the slightly longer procedure B, serious interference was not encountered from any metal in amounts up tu 50 mg. For practical purposes procedure B can be considered specific for thallium. As little as 10 μg of thallium in 25 g of liver could be determined. Deux variantes sont proposées pour le dosage du thallium dans des substances biologiques. Aprés minéralisation et extraction, le thallium est dosé absorptiométriquement sous forme de dithizonate, L'un de ces procédés est moins rapide que l'autre; mais il peut être considére pratiquement comme spécitique. Es werden zwei Varianten einer Methode beschrieben zur Bestimmung von Thallium in biologischem Material. Nach Zerstörung der organischen Substanz wird das Thalliúm als Chlorid extrahiert und als Dithizoonat absorptiometrisch bestimmt. Die eine Variante benötigt etwas mehr Zeitaufwand, kann aber als spezifisch betrachtet werden." @default.
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- W2060478606 date "1959-01-01" @default.
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- W2060478606 title "Determination of thallium in biological material" @default.
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- W2060478606 doi "https://doi.org/10.1016/0003-2670(59)80198-7" @default.
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