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- W2060478889 abstract "This paper provides a novel route to prepare silica monoliths with hierarchical porous structure via freeze drying. In this method, macroporous silica monoliths were first produced by freeze-drying and calcination. By adjusting the concentration of cetyltrimethylammonium bromide in ethylsilicate, a layer of mesoporous thin film was attached on the macroporous silica monolith. The structural characterization of the hierarchical porous monoliths were studied by field emission scanning electron microscopy, mercury porosimeter and nitrogen adsorption-desorption techniques (BET). It turned out that the pore distribution of the obtained monoliths was ranged from 3.72 nm to 23.21nm and the maximum specific surface area calculated from BET was about 288 m 2/ g, which indicated the existence of hierarchical structure in the obtained material." @default.
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- W2060478889 date "2015-03-01" @default.
- W2060478889 modified "2023-09-24" @default.
- W2060478889 title "Fabrication of Silica Monoliths with Hierarchically Porous Structure from Freeze-Drying" @default.
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- W2060478889 doi "https://doi.org/10.4028/www.scientific.net/msf.814.76" @default.
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