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- W2060483639 abstract "Treatment of [MO2Cl2·(DME)] (M = Mo, W; DME = 1,2-dimethoxyethane) with the lithium reagents LiLn [L1 = −N(SiMe3)(2-C5H3N-6-Me), L2 = −N(SiButMe2)(2-C5H3N-6-Me), L3 = −N(SiButPh2)(2-C5H3N-6-Me)] afforded the corresponding cis-dioxo-Mo(VI) amido complexes [MoO2(Ln)2] (Ln = L11, Ln = L22, Ln = L33) and cis-dioxo-W(VI) amido complexes [WO2(Ln)2] (Ln = L14, Ln = L25, Ln = L36). X-Ray crystallography shows that compounds 1, 2, 4 and 5 are mononuclear with the amido ligands bound to the metal centres in a N,N-chelating fashion forming highly strained four-membered metallacyclic rings with biting angles Namido–M–Npy around 60°. The Mo–Namido and W–Namido distances are comparable which fall in the range of 2.070–2.081 Å." @default.
- W2060483639 created "2016-06-24" @default.
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- W2060483639 date "2000-01-01" @default.
- W2060483639 modified "2023-10-17" @default.
- W2060483639 title "Synthesis and structures of dioxo-Mo(VI) and -W(VI) amides" @default.
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- W2060483639 doi "https://doi.org/10.1039/a907811h" @default.
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