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• W2060588520 abstract "Abstract The crystal structure of high-quality single crystals of YBa 2 Cu 3 O 6 + x grown in zirconia curcibles was studied systematically versus oxygen concentration by four-circle neutron diffraction at room temperature. The oxygen contents ranged from x = 0.18 (insulating, tetragonal phase) to x = 0.96 (superconducting, orthorhombic phase). In the orthorhombic phase, both twinned and detwinned samples were measured. A detailed discussion is presented of the systematic changes taking place in the atomic positions and Debye-Waller factors as the oxygen content is varied. Some qualitative highlights are that one can identify two distinct regions within the unit cell: the characteristics of the atoms near the CuO x basal plane are essentially driven by the effect of oxygen addition, whereas near the CuO 2 bilayer, the trends are more subtle and presumably dominated by charge transfer and bond-distance effects. Also, there is neither an abrupt change of the apical-oxygen position at the orthorhombic to tetragonal transition, nor is there any indication of depletion of the atomic sites except for the chain-site oxygen. The superconducting critical temperatures or Neel temperatures, as well as the existence of oxygen-ordered superstructures are reported." @default.
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• W2060588520 date "1996-02-01" @default.
• W2060588520 modified "2023-10-06" @default.
• W2060588520 title "Neutron-scattering determination of the structural parameters versus oxygen content of YBa2Cu3O6+x single crystals" @default.
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• W2060588520 doi "https://doi.org/10.1016/0921-4534(95)00674-5" @default.
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