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- W2060758203 abstract "This study describes a one-pot sol–gel method for the synthesis of Ag/TiO2 nanocomposite powders. TEM images showed that the Ag clusters formed with this method are highly dispersed on the surface of TiO2 nanoparticles. UV/visible spectroscopy results indicated that [BMIM][PF6], an imidazolium-based room-temperature ionic liquid, strongly inhibited the formation and growth of Ag clusters in N,N-dimethylformamide (DMF) solvent. This made it possible to prepare a stable stock solution containing AgNO3–[BMIM][PF6]–DMF. Dilution of the stock solution followed by hydrolysis resulted in a gel that was processed to produce Ag/TiO2 nanocomposites containing Ag clusters with average size smaller than 3 nm. XPS results indicated that the silver species exist predominantly in the metallic form. Because of the high dispersion and controlled size of the Ag clusters, the Ag/TiO2 nanocomposites demonstrated excellent catalytic performance in the aqueous phase reduction of methylene blue and the hydrogenation of 4-nitrophenol using NaBH4 as the reducing agent." @default.
- W2060758203 created "2016-06-24" @default.
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- W2060758203 date "2009-01-01" @default.
- W2060758203 modified "2023-10-01" @default.
- W2060758203 title "Ionic liquid-facilitated synthesis and catalytic activity of highly dispersed Ag nanoclusters supported on TiO2" @default.
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- W2060758203 doi "https://doi.org/10.1039/b910610c" @default.
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