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• W2060829596 abstract "In this article, we report the synthesis of methylene-bridged periodic mesoporous organosilicas (PMOs) of the SBA-15 type. The materials were characterized by SAXS, BET, NMR, FESEM, and TEM. It was found that the synthesis of methylene-bridged SBA-15 PMOs requires more rigorous conditions than that of SBA-15 PMOs bearing organic bridges other than methylene. A mild acidic environment, which slows down the hydrolysis and condensation rates of the precursor, with the assistance of a salt, which enhances precursor−template interaction, should be used to synthesize high-quality large-pore methylene-bridged PMOs. We attributed this to the fast hydrolysis and condensation rates and the rigid backbone of precursor 1,2-bis(triethoxysilyl)methylene. By examining and comparing the synthesis of three large-pore PMOs with different bridges, we concluded that the inductive, bridging, and conformation effects of the organic bridging group play an important role in the synthesis of large-pore PMO materials." @default.
• W2060829596 created "2016-06-24" @default.
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• W2060829596 date "2006-01-21" @default.
• W2060829596 modified "2023-10-14" @default.
• W2060829596 title "Synthesis of Large-Pore Methylene-Bridged Periodic Mesoporous Organosilicas and Its Implications" @default.
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• W2060829596 doi "https://doi.org/10.1021/jp0561120" @default.
• W2060829596 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/16471868" @default.
• W2060829596 hasPublicationYear "2006" @default.
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