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- W2060864292 abstract "Sephadex G-15 gel filtration chromatography (GFC) studies of supernatants from hydrosols prepared at SiAl ratios from 3.331 to 13.321 are reported. The GFC profiles exhibit two well-resolved peaks at Kav = 0.00 and 0.95. Based on the GFC behavior of known silicate complexes, the first eluted peak (Kav = 0.00) is assigned to polymeric complexes with molecular weights larger than the octasilicate ion but less than 2000 Da, while the second peak (Kav = 0.95) contains monomeric silicates. The polymeric/monomeric species content of chromatographed samples was dependent on the initial hydrosol SiAl ratio and reactant concentrations. Supernatants from low concentration hydrosols of SiAl ratio 6.661 showed the highest polymeric peak content with SiAl ratios of 71 to 91. Detailed chemical analyses and Sephadex G-15 GFC studies of 6.661 ratio SiAl hydrosol supernatants are also reported in order to clarify the influences of various synthesis parameters on the formation of soluble polymeric aluminosilicate complexes. Hydrosols prepared in the pH range 6–8 with a SiAl ratio of 6.661 showed the highest levels of polymeric aluminosilicate complexes with SiAl ratios from 71 to 121 and molecular weights between 800 and 1500 Da. A chemical model to describe the influence of these synthesis parameters together with plausible structures for the soluble aluminosilicates is presented." @default.
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- W2060864292 date "1992-07-01" @default.
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- W2060864292 title "Gel filtration chromatography of supernatants from aluminum silicate hydrosols of ratios from 3.33/1 to 13.32/1" @default.
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- W2060864292 doi "https://doi.org/10.1016/0021-9797(92)90481-z" @default.
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