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- W2061171241 abstract "Abstract The intercalation and deintercalation processes for nearly stoichiometric 1T-TaS 2 have been investigated by X-ray powder diffraction, thermogravimetric analysis, differential scanning calorimetry, and mass spectrometry. The maximum ammonia stoichiometry that has been prepared for a 4-month reaction time is (NH + 4 ) 0.06 (NH 3 ) 0.07 (1T-TaS 2 ) 0.06− . The reaction mechanism can be accounted for within a redox-rearrangement model in which part of the NH 3 is oxidized to NH + 4 upon intercalation, with the NH + 4 decomposing at the host-layer edges to liberate NH 3 and H 2 upon deintercalation. All intercalation compounds prepared could be deintercalated at relatively low temperatures. The intercalates retained some 1T-TaS 2 host material, which may be associated with the rather low concentration of intercalant combined with intercalation reaction fronts that only partially penetrate the host in a nucleation and growth process. This study indicates that ammoniated 1T-TaS 2 is a unique redox-rearrangement intercalation system." @default.
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- W2061171241 date "1999-06-01" @default.
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- W2061171241 title "Intercalation and Deintercalation Processes for Ammoniated 1T-TaS2" @default.
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- W2061171241 doi "https://doi.org/10.1006/jssc.1999.8293" @default.
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