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- W2061178536 abstract "Abstract Well‐defined poly(ferrocenyldimethylgermane) homopolymers PFDMG [ $overline M _{rm n} $ = 18 800–33 700, degree of polymerization ( $overline {DP} _{rm n} $ ) = 66–117, polydispersity index (PDI) = 1.02–1.05] and polyisoprene‐ block ‐poly(ferrocenyldimethylgermane) diblock copolymers (PI x ‐ b ‐PFDMG y , for 6 , x / y = 359:23, volume fraction, ϕ PFDMG = 0.14, PDI = 1.04; for 7 , x / y = 337:56, ϕ PFDMG = 0.29, PDI = 1.04) have been prepared by anionic ring‐opening polymerization. The polymer morphology and thermal transition behaviour of PFDMG 5 ( $overline M _{rm n} $ = 18 800, $overline {DP} _{rm n} $ = 66, PDI = 1.02) have been investigated by wide‐angle X‐ray scattering (WAXS) and differential scanning calorimetry (DSC), respectively. Both studies suggest that PFDMG 5 possesses similar crystallization behaviour to its Group 14 analogue, poly(ferrocenyldimethylsilane). Transmission electron microscopy (TEM) images of the solid state thin films of the diblock copolymers 6 ( ϕ PFDMG = 0.14) and 7 ( ϕ PFDMG = 0.29) show microphase separated structures of spherical or cylindrical PFDMG domains in a PI matrix respectively. Furthermore, these morphologies can be preserved after selective plasma etching of the PI block. magnified image" @default.
- W2061178536 created "2016-06-24" @default.
- W2061178536 creator A5005835981 @default.
- W2061178536 creator A5076582889 @default.
- W2061178536 date "2009-07-21" @default.
- W2061178536 modified "2023-10-14" @default.
- W2061178536 title "Anionic Ring‐Opening Polymerization of a Germanium‐Bridged [1]Ferrocenophane: Synthesis and Morphology of Well‐Defined Polyferrocenylgermane Homopolymers and Block Copolymers" @default.
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- W2061178536 doi "https://doi.org/10.1002/macp.200900089" @default.
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