FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2061367164> ?p ?o ?g. }

• W2061367164 endingPage "276" @default.
• W2061367164 startingPage "268" @default.
• W2061367164 abstract "Abstract In order to improve the economic sustainability of the Jatropha-biofuel chain, seed cake detoxification and utilization of ‘non toxic’ Jatropa curcas accessions are the main activities pursued with the aim of using J. curcas seed cake in animal feed. Given this growing interest, a robust and reliable method for phorbol esters (PEs) determination is necessary. HPLC-UV is a well-established method to detect and quantify the PEs content in Jatropha seeds and related products, but it seems to be unsuitable for more complex matrices like Jatropha leaves and animal tissues, due to the presence of interfering compounds. The objective of this work was to develop and optimize a LC–MS/MS method for the quantitative determination of PEs in seeds and leaves of J. curcas L. plants from Ghana and Mexico and in liver (as an organ with the function of accumulation) from goats fed with PEs in their diet. The HPLC-UV analysis evidenced five chromatographic peaks in the toxic seed kernels corresponding to the factors C1, C2, C3, C6 and C4–C5, respectively, with a PEs concentration of about 5100 μg/g (as TPA equivalent). No PEs related peaks were detected in Mexican kernel seeds while in the case of leaves and liver the analysis was hampered by the presence of interfering compounds. The toxic kernel seed extract was used as a standard solution for the PEs quantitation in leaves and liver samples by LC–MS/MS, with the standard addition method. The most intense MRM transitions used to quantify and qualify the PEs were: 675 → 311, 693 → 311, and 293 → 265 m/z. The LC–MS/MS method with a LOD and a LOQ of 0.07 and 0.21 μg/g, respectively, resulted in more sensitivity and selectivity than the HPLC-UV method. All three MRM transitions were present in Ghanaian toxic kernel seed, while no peaks were present in the supposed non-toxic Mexican kernel seed. PEs concentration in the leaves of toxic Ghanaian accession resulted in about 1/10 of that in the kernel, while no PEs peaks were found in the J. curcas leaves from Mexico and in liver samples." @default.
• W2061367164 created "2016-06-24" @default.
• W2061367164 creator A5003776110 @default.
• W2061367164 creator A5007420382 @default.
• W2061367164 creator A5033958739 @default.
• W2061367164 creator A5064517733 @default.
• W2061367164 creator A5065229036 @default.
• W2061367164 creator A5074277610 @default.
• W2061367164 creator A5074996453 @default.
• W2061367164 date "2014-08-01" @default.
• W2061367164 modified "2023-09-27" @default.
• W2061367164 title "Determination of phorbol esters in seeds and leaves of Jatropha curcas and in animal tissue by high-performance liquid chromatography tandem mass spectrometry" @default.
• W2061367164 cites W1501710458 @default.
• W2061367164 cites W1525932745 @default.
• W2061367164 cites W1965585950 @default.
• W2061367164 cites W1999868048 @default.
• W2061367164 cites W2001083420 @default.
• W2061367164 cites W2005313014 @default.
• W2061367164 cites W2034252021 @default.
• W2061367164 cites W2034712687 @default.
• W2061367164 cites W2040356743 @default.
• W2061367164 cites W2045238428 @default.
• W2061367164 cites W2059250885 @default.
• W2061367164 cites W2063744211 @default.
• W2061367164 cites W2081018688 @default.
• W2061367164 cites W2081942920 @default.
• W2061367164 cites W2083791241 @default.
• W2061367164 cites W2088142354 @default.
• W2061367164 cites W2092555951 @default.
• W2061367164 cites W2096165284 @default.
• W2061367164 cites W2102294596 @default.
• W2061367164 cites W2114840302 @default.
• W2061367164 cites W2115894894 @default.
• W2061367164 cites W2124616078 @default.
• W2061367164 cites W2132208042 @default.
• W2061367164 cites W2134579141 @default.
• W2061367164 cites W2138048463 @default.
• W2061367164 cites W2153281302 @default.
• W2061367164 cites W2171736964 @default.
• W2061367164 doi "https://doi.org/10.1016/j.indcrop.2014.05.034" @default.
• W2061367164 hasPublicationYear "2014" @default.
• W2061367164 type Work @default.
• W2061367164 sameAs 2061367164 @default.
• W2061367164 citedByCount "28" @default.
• W2061367164 countsByYear W20613671642015 @default.
• W2061367164 countsByYear W20613671642016 @default.
• W2061367164 countsByYear W20613671642017 @default.
• W2061367164 countsByYear W20613671642018 @default.
• W2061367164 countsByYear W20613671642019 @default.
• W2061367164 countsByYear W20613671642021 @default.
• W2061367164 countsByYear W20613671642022 @default.
• W2061367164 crossrefType "journal-article" @default.
• W2061367164 hasAuthorship W2061367164A5003776110 @default.
• W2061367164 hasAuthorship W2061367164A5007420382 @default.
• W2061367164 hasAuthorship W2061367164A5033958739 @default.
• W2061367164 hasAuthorship W2061367164A5064517733 @default.
• W2061367164 hasAuthorship W2061367164A5065229036 @default.
• W2061367164 hasAuthorship W2061367164A5074277610 @default.
• W2061367164 hasAuthorship W2061367164A5074996453 @default.
• W2061367164 hasConcept C159985019 @default.
• W2061367164 hasConcept C161790260 @default.
• W2061367164 hasConcept C162356407 @default.
• W2061367164 hasConcept C185592680 @default.
• W2061367164 hasConcept C192562407 @default.
• W2061367164 hasConcept C2777247137 @default.
• W2061367164 hasConcept C2777814067 @default.
• W2061367164 hasConcept C2778733479 @default.
• W2061367164 hasConcept C31827203 @default.
• W2061367164 hasConcept C43617362 @default.
• W2061367164 hasConcept C52896960 @default.
• W2061367164 hasConcept C55493867 @default.
• W2061367164 hasConcept C59822182 @default.
• W2061367164 hasConcept C64489805 @default.
• W2061367164 hasConcept C86803240 @default.
• W2061367164 hasConceptScore W2061367164C159985019 @default.
• W2061367164 hasConceptScore W2061367164C161790260 @default.
• W2061367164 hasConceptScore W2061367164C162356407 @default.
• W2061367164 hasConceptScore W2061367164C185592680 @default.
• W2061367164 hasConceptScore W2061367164C192562407 @default.
• W2061367164 hasConceptScore W2061367164C2777247137 @default.
• W2061367164 hasConceptScore W2061367164C2777814067 @default.
• W2061367164 hasConceptScore W2061367164C2778733479 @default.
• W2061367164 hasConceptScore W2061367164C31827203 @default.
• W2061367164 hasConceptScore W2061367164C43617362 @default.
• W2061367164 hasConceptScore W2061367164C52896960 @default.
• W2061367164 hasConceptScore W2061367164C55493867 @default.
• W2061367164 hasConceptScore W2061367164C59822182 @default.
• W2061367164 hasConceptScore W2061367164C64489805 @default.
• W2061367164 hasConceptScore W2061367164C86803240 @default.
• W2061367164 hasLocation W20613671641 @default.
• W2061367164 hasOpenAccess W2061367164 @default.
• W2061367164 hasPrimaryLocation W20613671641 @default.
• W2061367164 hasRelatedWork W1969559554 @default.
• W2061367164 hasRelatedWork W1973261120 @default.
• W2061367164 hasRelatedWork W2018070089 @default.
• W2061367164 hasRelatedWork W2046598237 @default.
• W2061367164 hasRelatedWork W2115218143 @default.
• W2061367164 hasRelatedWork W2346859668 @default.

• next