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• W2061574628 abstract "The (+/−)-cis-5-arylcarbamoyl-2-ethoxycarbonylpyrrolidines 6a–g were firstly synthesized in 53–64% yields by using meso-diethyl-2,5-dibromoadipate 3 and (S)-(−)-1-phenylethylamine in three steps. The diastereomeric mixture (S;2S,5R)-(−)-7 and (S;2R,5S)-(+)-8 were prepared by the Grignard reaction and separated by a flash column chromatography in 29 and 52% yields. The absolute configurations of (+)-8 was confirmed by X-ray crystallographic analysis and the enantiopure pyrrolidines (2S,5R)-(−)-9/(2R,5S)-(+)-9 and (2S,5R)-(−)-10/(2R,5S)-(+)-10 were obtained in good yields. Chirality, 2007. © 2007 Wiley-Liss, Inc." @default.
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• W2061574628 date "2007-07-01" @default.
• W2061574628 modified "2023-09-26" @default.
• W2061574628 title "Facile synthetic route to enantiopure unsymmetric<i>cis</i>-2,5-disubstituted pyrrolidines" @default.
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• W2061574628 doi "https://doi.org/10.1002/chir.20424" @default.
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