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- W2061670039 abstract "The structure was solved by the Patterson method and suc- cessive Fourier electron density difference maps, and refined by full-matrix least-squares procedures with anisotropic tem- perature factors for all non-H atoms. The positions of all H atoms were generated geometrically in the final stages of re- finement. Anomalous-dispersion corrections were taken from Cromer & Liberman (1970) for non-H atoms and from Stew- art, Davidson & Simpson (1965) for H atoms. Programs used were SDP (Enraf-Nonius, 1985), SHELX76 (Sheldrick, 1976) and ORTEP (Johnson, 1965). This work has received partial support from CNPq, FAPESP and FINEE which are hereby gratefully ac- knowledged. Abstract The title compound, (6-(4-aminobenzyl)- 1,11-diaza-4,8- diazanidacyclotetradecane-5,7-dione(2- )-/~4N 1,4,8,11 ) _ nickel(II), (Ni(C17H25N502)), has mirror symmetry with Ni--N(amide) and Ni--N(amine) bond distances of 1.862(5) and 1.925 (5)/~, respectively. The aromatic ring of the side chain is tipped 21.3 (3) ° towards the plane containing the Ni and four N atoms. The distance from the Ni atom to the center of the aromatic ring is 3.551 (5) A." @default.
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- W2061670039 date "1995-04-15" @default.
- W2061670039 modified "2023-09-25" @default.
- W2061670039 title "An Aminobenzyldioxocyclam Nickel(II) Complex" @default.
- W2061670039 doi "https://doi.org/10.1107/s0108270194011753" @default.
- W2061670039 hasPublicationYear "1995" @default.
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