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- W2061839573 abstract "The direct electrochemical reduction of solid titanium dioxide (TiO 2 ) is conducted in [BMIM]BF 4 -CaCl 2 ionic liquid (IL) at 100 °C using sintered TiO 2 as cathode and graphite rod as anode at an electrolysis potential of 3.2 V. Cyclic voltammetry is used to investigate the mechanism and feasibility of the direct electrochemical reduction of solid TiO 2 in [BMIM]BF 4 -CaCl 2 IL at 100 °C. The surface morphologies of the cathode are examined by scanning electron microscopy（SEM）. The crystal phase structure of the cathode is examined using a D8 Advance X-ray diffractometer(XRD). The results indicate that the direct electrochemical reduction of solid TiO 2 in [BMIM]BF 4 -CaCl 2 IL is feasible. A significant increase in conductivity is obtained by doping graphite into the cathode, thereby enhancing deoxidation. TiO 2 reduction is conducted step by step, from outside to inside, and from high to low valence variation." @default.
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- W2061839573 date "2014-01-01" @default.
- W2061839573 modified "2023-10-04" @default.
- W2061839573 title "Direct Electrochemical Reduction of Solid TiO<sub>2</sub> in [BMIM]BF<sub>4</sub>-CaCl<sub>2</sub> Ionic Liquid" @default.
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- W2061839573 doi "https://doi.org/10.4028/www.scientific.net/amm.492.248" @default.
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