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- W2061864467 abstract "An electron diffraction structure analysis was carried out on benzene sulphonyl chloride, C6H5SO2Cl, utilizing data from concurrent vibrational spectroscopie calculations. The following bond lengths (ra parameters): C-H 1.14 ± 0.03 Å, C-C 1.403 ± 0.010 Å, S-O 1.417 ± 0.012 Å, C-S 1.764 ± 0.009 Å and S-Cl 2.047 ± 0.008 Å and bond angles (rα parameters): C-S-C1 100.9 ± 2.0°, C-S-O 110.0 ± 2.5°, O-S-O 122.5 ± 3.6° and O-S-Cl 105.5 ± 1.8° were determined for an asymmetric model in which the benzene ring is rotated by 75.3 ± 5.0° relative to the plane containing the sulphur-chlorine bond and bisecting the O-S-O angle. The experimental data could equally well be approximated by a symmetric model with the benzene ring perpendicular to the reference plane described previously, if a particularly large amplitude of vibration was associated with the shortest rotation-dependent carbon-chlorine distance. The bond configuration around the sulphur atom in benzene sulphonyl chloride is consistent with the structural variations observed for a series of sulphone molecules." @default.
- W2061864467 created "2016-06-24" @default.
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- W2061864467 date "1976-02-01" @default.
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- W2061864467 title "The molecular structure of benzene sulphonyl chloride" @default.
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- W2061864467 doi "https://doi.org/10.1016/0022-2860(76)87013-5" @default.
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