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- W2061894625 abstract "Abstract Selective oxidation of one (trans to N) carbonyl group in [Rh(8-Oxiquinolinato)(CO)2] with stoichiometric amount of Me3NO in MeCN produces a solution containing [Rh(Oxq)(CO)(Me3N)] and [Rh(Oxq)(CO)(MeCN)]. The ammonia complex, [Rh(Oxq)(CO)(NH3)], has been prepared by action of NH3 gas on this solution and characterized by IR, 1H and 13C NMR, and X-ray data. Spectral parameters, ν(CO), δ 13C, and 1J(CRh), were measured in situ for a series of complexes [Rh(Oxq)(CO)(L)] (L = NAlk3, Py, PBu3, PPh3, P(OPh)3, C8H14) formed upon action of L on [Rh(Oxq)(CO)(NH3)] in THF. A new ν(CO) and δ 13C based scale of σ-donor/π-acceptor properties of ligands L is proposed including NH3 and CO as the natural endpoints." @default.
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- W2061894625 date "2007-12-01" @default.
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- W2061894625 title "First examples of [Rh(Bident)(CO)(L)] complexes where L is N-donor ligand: Molecular structure of [Rh(8-Oxiquinolinato)(CO)(NH3)]" @default.
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- W2061894625 doi "https://doi.org/10.1016/j.jorganchem.2007.09.022" @default.
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