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- W2061917394 abstract "Die säulenchromatographische Aminosäure-Analyse wurde im Gegenwart von Schwermetall-Kationen durchgeführt. Im Elutionsdiagramm der Aminosäuren wurden die Positionen der Banden von Fe8+, Cu2+ und Ni2+ festgelegt. Der Fe8_+-Peak überlappt Cysteinsäure. Im Gegensatz zu Fe3+ werden Cu2+ und Ni2+ in Form stark verbreiterter Banden eluiert, die unter Valin und Methionin, bzw. Methionin, Isoleucin und Leucin liegen. Bei der Anfärbung der Aminosäuren Cysteinsäure, Cystin, Leucin und Histidin mit Ninhydrin-Hydrindatin bewirkt Fe3+-Zusatz eine signifikante Erhöhung der Extinktionswerte. Auf den durch Fe3+ verursachten Fehler bei der säulenchromatographischen Cysteinsäure-Bestimmung wird hingewiesen.Amino acids were analyzed by ion-exchange chromatography in the presence of heavy metal cations. The positions of Fe3+, Cu2+ and Ni2+ were determined under conditions used for the separation of amino acids on Amberlite CG 120. The Fe3+-peak is eluted together with cystein acid. Valine and methionine overlap with Cu2+, while the position of Ni2+ coincides with that of methionine, isoleucine, and leucine. Iron significantly increases the extinction values of the reaction products of the amino acids cystein acid, cystine, leucine and histidine with ninhydrin-hydrindantin. It has been shown that iron may cause erroneous results in the column chromatographic determination of cystein acid." @default.
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- W2061917394 date "2000-09-01" @default.
- W2061917394 modified "2023-09-27" @default.
- W2061917394 title "PPI deficits in antipsychotic-treated, chronic schizophrenic patients" @default.
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- W2061917394 doi "https://doi.org/10.1016/s0924-977x(00)80376-4" @default.
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