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• W2061965929 abstract "The synthesis of a new ligand system in which two amides are coupled via a rigid phenylene spacer is readily accomplished in a high-yield, single-step reaction. The dilithio salt (NO)2Li2(THF)x reacts with Ti(NR2)4 (R = Me, Et) to yield the titanium amides [(NO)2Ti(NR2)2]2. The latter react with excess Me3SiCl to produce the dichloride (NO)2TiCl2, which was also obtained by the reaction of [(NO)2Ti(NMe2)2]2 with TiCl4(THF)2 in refluxing toluene, and in a lower-yielding route, by salt metathesis between the dilithio salt and TiCl4(THF)2." @default.
• W2061965929 created "2016-06-24" @default.
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• W2061965929 date "2001-10-03" @default.
• W2061965929 modified "2023-10-10" @default.
• W2061965929 title "Synthesis and Structure of a Linked-Bis(amidate) Ligand and Some Complexes with Titanium" @default.
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• W2061965929 doi "https://doi.org/10.1021/ic010533o" @default.
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