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- W2061978556 abstract "The compound SbOPO4 was prepared two different ways: thermal decomposition of the phosphatoantimonic acid HSbP2O8 · xH2O or synthesis at 1173 K from a stoichiometric mixture of Sb2O5 · xH2O and (NH4)H2PO4. At 1218 K SbOPO4 undergoes a deoxidation process leading to the Sb(III) phosphate SbPO4. SbOPO4 crystallizes in the monoclinic system, space group C2c with a = 6.791(1)Å, b = 8.033(1) Å, c = 7.046(1) Å, β = 115.90(1)°, Z = 4. The structure was determined from 481 reflexions collected on a NONIUS CAD4 automatic diffractometer with MoKα radiation. The final R index and weighted Rw index are 0.028 and 0.035, respectively. The structure is built up from chains of corner-shared SbO6 octahedra, parallel to the c axis, crosslinked by corner-shared tetrahedra. Each phosphate group is bonded to four SbO6 octahedra of which two belong to the same chain. This structure is closely related to that of β-VOSO4 and β-VOPO4." @default.
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- W2061978556 date "1986-06-01" @default.
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- W2061978556 title "Synthesis, thermal stability, and crystal structure of antimony(V) phosphate SbOPO4" @default.
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- W2061978556 doi "https://doi.org/10.1016/0022-4596(86)90155-6" @default.
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