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• W2062027218 abstract "Optimized procedures were established for the determination of total Se, organic Se, Se(IV), and Se(VI) in human hair by means of hydride-generation atomic absorption spectrometry (HGAAS), respectively. Using this method, the total Se content in a hair sample was determined through pretreating the sample with nitric acid-perchloric acid, and then reducing Se(VI) to Se(IV) with 6.0 mol dm-3 hydrochloric acid; however, for individual Se(IV), Se(VI) or soluble Se, after the hair sample was immersed into water and disrupted ultrasonically for 8 h at room temperature, 2,3-diaminonaphthalene (DAN) reagent was added to extract Se(IV). The sum of Se(IV) and Se(VI) was determined by extracting Se(IV) after reducing all of the Se(VI) into Se(IV) with the addition of potassium bromide. Se(VI) was obtained by subtracting Se(IV) from the sum of Se(IV) and Se(VI). The content of organic Se in’ the hair sample was calculated by subtracting Se(IV)+Se(VI) from the total Se. The detection limit of the method was 0.3 ngSe cm-3, and the average precision (relative standard deviation) was less than 5% (n=6)." @default.
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• W2062027218 date "1997-04-01" @default.
• W2062027218 modified "2023-10-17" @default.
• W2062027218 title "Quantitative Analysis of Human Hair for Selenium(IV), Selenium(VI) and Total Selenium by Hydride-Generation Atomic Absorption Spectrometry" @default.
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• W2062027218 doi "https://doi.org/10.2116/analsci.13.195" @default.
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