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• W2062072009 abstract "Abstract Green rusts, GRs, can act as both sorbents and reductants towards selected pollutants. Organo-GRs are expected to combine these properties with a high affinity for hydrophobic substances. A novel organo-GR, GR LAS , was synthesized by incorporating a mixture of linear alkylbenzenesulphonates (LAS) into the interlayer space of synthetic sulphate green rust, GR SO4 . Mössbauer analysis of GR LAS indicates that the structure of the organo-GR is very similar to that of the initial GR SO4 with regard to the Fe II /Fe III ratio and local coordination of Fe atoms. X-ray diffraction demonstrates that the GR LAS formed was well ordered, although a mixture of surfactant was used for intercalation. The basal spacings of the GR LAS and the kinetics of the ion-exchange process were dependent on the initial surfactant loading; basal spacings of ~2.85 nm were obtained at LAS solution concentrations >10 mM. The ratio LAS adsorbed /SO 4 2– desorbed significantly exceeded the stoichiometric ratio of 2 during the initial part of the ion-exchange process ( t = 5 h). However, this ratio was reached progressively with time. GR SO4 preferentially sorbed LAS homologues with long alkyl chains over short ones. Carbon tetrachloride was successfully adsorbed into GR LAS . The adsorption isotherm was linear with a distribution coefficient, K d , of 505±19 litre kg –1 ." @default.
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• W2062072009 date "2007-09-01" @default.
• W2062072009 modified "2023-10-16" @default.
• W2062072009 title "Synthesis of linear alkylbenzene sulphonate intercalated iron(II) iron(III) hydroxide sulphate (green rust) and adsorption of carbon tetrachloride" @default.
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• W2062072009 doi "https://doi.org/10.1180/claymin.2007.042.3.04" @default.
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