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- W2062432007 abstract "Abstract A novel ethylenediamine-gallium phosphate, formulated as Ga(H2NCH2CH2NH2)2PO4·2H2O, was synthesized under hydrothermal conditions. The crystal structure, including hydrogen positions, was determined using single-crystal X-ray diffraction data (monoclinic, a=9.4886(3) A, b=6.0374(2) A, c=10.2874(3) A, and β=104.226(3)°, space group Pc) and the bulk was characterized by chemical (Ga–P–C–H–N) and thermal analysis (TG–MS and DSC), including activation energy data of its thermo-oxidative degradation, powder X-ray diffraction (PXRD), solid-state nuclear magnetic resonance (SS-NMR) measurements, and transmission electron microscopy (TEM, SAED/NBD, and STEM BF-EDX). The crystal structure is built up of infinite zig-zag chains running along the c-axis, formed by vertex-shared {PO4} and {GaO2N4} polyhedra. The new compound is characterized by unusual four equatorial Ga–N bonds coming from two nonequivalent ethylenediamine molecules and exhibits strong blue emission at 430 nm (λex=350 nm) in the solid state at room temperature." @default.
- W2062432007 created "2016-06-24" @default.
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- W2062432007 date "2014-07-01" @default.
- W2062432007 modified "2023-09-27" @default.
- W2062432007 title "Novel ethylenediamine-gallium phosphate containing 6-fold coordinated gallium atoms with unusual four equatorial Ga–N bonds" @default.
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- W2062432007 doi "https://doi.org/10.1016/j.jssc.2014.03.024" @default.
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