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- W2062667572 abstract "Abstract The Tup fragments of tubulysins were synthesized with a tandem reaction as the key step, and unexpected diastereoselectivity was observed in the first Grignard addition stage. The coupling of the enolate of a thiazolyl ketone with chiral sulfinimines furnished the backbone of the Tuv fragment with over 100:1 d.r. and high yield. Thus, tubulysin U and C‐4 epi‐tubulysin U were prepared in a highly selective and efficient manner. The results of the MTT assay furthermore indicated that C‐4 epi‐tubulysin U maintained significant growth inhibition activities against several cancer cell lines." @default.
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- W2062667572 date "2013-04-10" @default.
- W2062667572 modified "2023-10-18" @default.
- W2062667572 title "Total Synthesis of Tubulysin U and Its C-4 Epimer" @default.
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- W2062667572 doi "https://doi.org/10.1002/asia.201300051" @default.
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