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- W2062893100 abstract "The bimetallic complexes fc(μ2-S)2TiCp2 (1, fc = 1,1‘-ferrocenyl, Cp = cyclopentadienyl) and fc(μ2-S2)(μ2-S)TiCp2 (2) were synthesized by reaction of fc(SH)2 with Cp2TiCl2, and from fcS3 and Cp2Ti(CO)2, respectively. The novel tetrasulfane fcS4 was obtained from 2 and SCl2. 1,3-Dithia[3]ferrocenophane fcS2CH2 was obtained from fc(SH)2 and CH2Cl2 in the presence of Cp2TiCl2 and KOH. The molecular and crystal structure of fcS2CH2 was determined by X-ray crystallography; the molecular symmetry is Cs. Electrochemical studies on the recently prepared ferrocenophanes fcS2-1-SO, fcS2-1-SO2, and fcS2-2-SO show that, with respect to fcS3, the progressive oxidation of the trisulfane bridge makes more and more difficult the fc/fc+ oxidation, whereas insertion of a Cp2Ti fragment exerts the opposite effect." @default.
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- W2062893100 date "2002-05-24" @default.
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- W2062893100 title "Synthetic and Electrochemical Studies on 1,1‘-Dithia-Substituted Derivatives of Ferrocene and Structure of 1,3-Dithia[3]ferrocenophane [Fe(C<sub>5</sub>H<sub>4</sub>S)<sub>2</sub>CH<sub>2</sub>]" @default.
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- W2062893100 doi "https://doi.org/10.1021/om020041z" @default.
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